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Métodos Analíticos EPA SERIES 8000-9000 |
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Métodos EPA |
Un método analítico
es un procedimiento usado para analizar una muestra para determinar la
identidad y concentración de un constituyente específico de la muestra.
Los métodos analíticos incluyen generalmente información sobre la toma,
transporte y almacenamiento de muestras; define procedimientos para
concentrar, separar, identificar y cuantificar los componentes incluidos
en la muestra; especifica qué criterios de control de calidad han de
alcanzar los datos analíticos y especifica como construir los informes
analíticos. Muchas agencias gobernativas, universidades y organizaciones de normalización desarrollan métodos analíticos. La Environmental Protection Agency de Estados Unidos es responsable en la evaluación de cada método analítico en función de su origen. Por ejemplo la "Office of Ground Water and Drinking Water" se responsabiliza en la evaluación de métodos analíticos desarrollados por esas organizaciones para el análisis de agua potable. La Oficina promulga, como aprobados, aquellos métodos que determina alcanzan las exigencia de la Agencia para el control de contaminantes orgánicos, inorgánicos, radio nucleares y microbiológicos. Actualmente, sólo pueden usarse métodos aprobados para el control de agua potable. Estos métodos se entiende que se usarán como una herramienta de referencia y proveen al usuario de la información necesaria sobre métodos analíticos aprobados para el control según normativa. |
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EPA Serie 8000 | Los Métodos de la Serie EPA 8000 ha sido diseñados para identificar contaminantes orgánicos en aguas continentales tal como prescribe la "Resource Recovery and Conservation Act (RCRA)". | ||
Método | Descripción | Tamaño | |
8000B | Determinative Chromatographic Separations | 248 Kb | |
8010B | Halogenated Volatile Organics by Gas Chromatography | 150 Kb | |
8011 | 1,2-Dibromoethane and 1,2-Dibromo-3-chloropropane by Microextraction and Gas Chromatography | 172 Kb | |
8015B | Nonhalogenated Organics Using GC/FID | 234 Kb | |
8015C | Nonhalogenated Organics by Gas Chromatography | 315 Kb | |
8020A | Aromatic Volatile Organics by Gas Chromatography | 165 Kb | |
8021B | Aromatic and Halogenated Volatiles by Gas Chromatography Using Photoionization and/or Electrolytic Conductivity Detectors | 130 Kb | |
8030A | Acrolein and Acrylonitrile by Gas Chromatography | 121 Kb | |
8031 | Acrylonitrile by Gas Chromatography | 77 Kb | |
8032A | Acrylamide by Gas Chromatography | 104 Kb | |
8033 | Acetonitrile by Gas Chromatography with Nitrogen-Phosphorus Detection | 73 Kb | |
8040 |
Phenols by Gas Chromatography |
205 Kb | |
8041 | Phenols by Gas Chromatography | ||
8041A | Phenols by Gas Chromatography | 133 Kb | |
8061A | Phthalate Esters by Gas Chromatography with Electron Capture Detection (GC/ECD) | 103 Kb | |
8070A | Nitrosamines by Gas Chromatography | 102 Kb | |
8080A | Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography | 348 Kb | |
8081A | Organochlorine Pesticides by Gas Chromatography | 298 Kb | |
8081B | Organochlorine Pesticides by Gas Chromatography | 309 Kb | |
8082 | Polychlorinated Biphenyls (PCBs) by Gas Chromatography | 265 Kb | |
8082A | Polychlorinated Biphenyls (PCBs) by Gas Chromatography | 376 Kb | |
8085 | Compound-Independent Elemental Quantitation of Pesticides by Gas Chromatography with GC/AED | 232 Kb | |
8091 | Nitroaromatics and Cyclic Ketones by Gas Chromatography | 116 Kb | |
8095 | Explosives by Gas Chromatography | 104 Kb | |
8100 | Polynuclear Aromatic Hydrocarbons | 207 Kb | |
8111 | Haloethers by Gas Chromatography | 87 Kb | |
8121 | Chlorinated Hydrocarbons by Gas Chromatography: Capillary Column Technique | 357 Kb | |
8131 | Aniline and Selected Derivatives by Gas Chromatography | 103 Kb | |
8141A | Organophosphorus Compounds by Gas Chromatography: Capillary Column Technique | 460 Kb | |
8141B | Organophosphorus Compounds by Gas Chromatography | 187 Kb | |
8151A | Chlorinated Herbicides by GC Using Methylation or Pentafluorobenzylation Derivatization | 228 Kb | |
8240B | Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) | 390 Kb | |
8260B | Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) | 444 Kb | |
8261 | Volatile Organic Compounds by Vacuum Distillation in Combination with Gas Chromatography/Mass Spectrometry (VD/GC/MS) | 292 Kb | |
8270C | Semivolatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) | 313 Kb | |
8270D | Semivolatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) | 374 Kb | |
8275A | Semivolatile Organic Compounds (PAHs and PCBs) in Soils/Sludges and Solid Wastes Using Thermal Extraction/Gas Chromatography/Mass Spectrometry (TE/GC/MS) | 151 Kb | |
8280A | The Analysis of Polychlorinated Dibenzo-p-Dioxins and Polychlorinated Dibenzofurans by High Resolution Gas Chromatography/Low Resolution Mass Spectrometry (HRGC/LRMS) | 269 Kb | |
8280B | The Analysis of Polychlorinated Dibenzodioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs) by High-Resolution Gas Chromatography/Low-Resolution Mass Spectrometry (HRGC/HRMS) | 172 Kb | |
8290 | Polychlorinated Dibenzodioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs) by High-Resolution Gas Chromatography/High-Resolution Mass Spectrometry (HRGC/HRMS) | 612 Kb | |
8290A | Polychlorinated Dibenzodioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs) by High-Resolution Gas Chromatography/High-Resolution Mass Spectrometry (HRGC/HRMS) | 261 Kb | |
8310 | Polynuclear Aromatic Hydrocarbons | 254 Kb | |
8315A | Determination of Carbonyl Compounds by High Performance Liquid Chromatography (HPLC) | 238 Kb | |
8316 | Acrylamide, Acrylonitrile and Acrolein by High Performance Liquid Chromatography (HPLC) | 70 Kb | |
8318 | N-Methylcarbamates by High Performance Liquid Chromatography (HPLC) | 213 Kb | |
8318A | N-Methylcarbamates by High Performance Liquid Chromatography (HPLC) | 125 Kb | |
8321A | Solvent Extractable Nonvolatile Compounds by High Performance Liquid Chromatography/Thermospray/Mass Spectrometry (HPLC/TS/MS) or Ultraviolet (UV) Detection | 239 Kb | |
8321B | Solvent Extractable Nonvolatile Compounds by High Performance Liquid Chromatography/Thermospray/Mass Spectrometry (HPLC/TS/MS) or Ultraviolet (UV) Detection | 147 Kb | |
8325 | Solvent Extractable Nonvolatile Compounds by High Performance Liquid Chromatography/Particle Beam/Mass Spectrometry (HPLC/PB/MS) | 141 Kb | |
8330 | Nitroaromatics and Nitramines by High Performance Liquid Chromatography (HPLC) | 285 Kb | |
8330A | Nitroaromatics and Nitramines by High Performance Liquid Chromatography (HPLC) | 83 Kb | |
8331 | Tetrazene by Reverse Phase High Performance Liquid Chromatography (HPLC) | 157 Kb | |
8332 | Nitroglycerine by High Performance Liquid Chromatography | 45 Kb | |
8410 | Gas Chromatography/Fourier Transform Infrared (GC/FT-IR) Spectrometry for Semivolatile Organics: Capillary Column | 210 Kb | |
8430 | Analysis of Bis(2-chloroethyl) Ether and Hydrolysis Products by Direct Aqueous Injection GC/FT-IR | 79 Kb | |
8440 | Total Recoverable Petroleum Hydrocarbons by Infrared Spectrophotometry | 48 Kb | |
8510 | Colorimetric Screening Procedure for RDX and HMX in soil | 63 Kb | |
8515 | Colorimetric Screening Procedure for Trinitrotoluene (TNT) in soil | 22 Kb | |
8520 | Continous Measurement of Formaldehyde in Ambient Air | 199 Kb | |
8535 | Screening Procedure for Total Volatile Organic Halides in Water | 86 Kb | |
8540 | Pentachlorophenol in Soil by UV-Induced Colorimetry | 73 Kb | |
EPA Serie 9000 | Los Métodos EPA de la Serie 9000 se han diseñado para el control de contaminantes orgánicos, inorgánicos y otros parámetros en matrices varias mediante técnicas espectroscópicas. | ||
Método | Descripción | Tamaño | |
9000 | Determination of Water in Waste Materials by Karl Fischer Titration | 46 Kb | |
9001 | Determination of Water in Waste Materials by Quantitative Calcium Hydride Reaction | 42 Kb | |
9010C | Total and Amenable Cyanide: Distillation | 58 Kb | |
9012B | Total and Amenable Cyanide (Automated Colorimetric, with Off-Line Distillation) | 100 Kb | |
9013 | Cyanide Extraction Procedure for Solids and Oils | 157 Kb | |
9014 | Titrimetric and Manual Spectrophotometric Determinative Methods for Cyanide | 72 Kb | |
9020B | Total Organic Halides (TOX) | 190 Kb | |
9021 | Purgeable Organic Halides (POX) | 197 Kb | |
9022 | Total Organic Halides (TOX) by Neutron Activation Analysis | 248 Kb | |
9023 | Extractable Organic Halides (EOX) in Solids | 92 Kb | |
9030B | Acid-Soluble and Acid-Insoluble Sulfides: Distillation | 113 Kb | |
9031 | Extractable Sulfides | 316 Kb | |
9034 | Extractable Sulfides | 60 Kb | |
9035 | Sulfate (Colorimetric, Automated, Chloranilate) | 215 Kb | |
9036 | Sulfate (Colorimetric, Automated, Methylthymol Blue, AA II) | 225 Kb | |
9038 | Sulfate (Turbidimetric) | 186 Kb | |
9040C | pH Electrometric Measurement | 25 Kb | |
9041A | pH Paper Method | 66 Kb | |
9045D | Soil and Waste pH | 30 Kb | |
9050A | Specific Conductance | 31 Kb | |
9056A | Determination of Inorganic Anions by Ion Chromatography | 280 Kb | |
9057 | Determination of Chloride from HCl/Cl2 Emission Sampling Train (Methods 0050 and 0051) by Anion Chromatography | 44 Kb | |
9060A | Total Organic Carbon | 26 Kb | |
9065 | Phenolics (Spectrophotometric, Manual 4-AAP with Distillation) | 212 Kb | |
9066 | Phenolics (Colorimetric, Automated 4-AAP with Distillation) | 223 Kb | |
9067 | Phenolics (Spectrophotometric, MBTH with Distillation) | 160 Kb | |
9070A | n-Hexane Extractable Material (HEM) for Aqueous Samples | 16 Kb | |
9071B | n-Hexane Extractable Material (HEM) for Sludge, Sediment, and Solid Samples | 82 Kb | |
9074 | Turbidimetric Screening Method for Total Recoverable Petroleum Hydrocarbons in Soil | 85 Kb | |
9075 | Test Method for Total Chlorine in New and Used Petroleum Products by X-Ray Fluorescence Spectrometry (XRF) | 62 Kb | |
9076 | Test Method for Total Chlorine in New and Used Petroleum Products by Oxidative Combustion and Microcoulometry | 81 Kb | |
9077 | Test Methods for Total Chlorine in New and Used Petroleum Products (Field Test Kit Methods) | 334 Kb | |
9078 | Screening Test Method for Polychlorinated Biphenyls in Soil | 32 Kb | |
9079 | Screening Test Method for Polychlorinated Biphenyls in Transformer Oil | 46 Kb | |
9080 | Cation-Exchange Capacity of Soils (Ammonium Acetate) | 266 Kb | |
9081 | Cation-Exchange Capacity of Soils (Sodium Acetate) | 135 Kb | |
9090A | Compatibility Test for Wastes and Membrane Liners | 611 Kb | |
9095B | Paint Filter Liquids Test | 28 Kb | |
9096 | Liquid Release Test (LRT) Procedure | 249 Kb | |
9100 | Saturated Hydraulic Conductivity, Saturated Leachate Conductivity, and Intrinsic Permeability | 866 Kb | |
9131 | Total Coliform: Multiple Tube Fermentation Technique | 301 Kb | |
9132 | Total Coliform: Membrane-Filter Technique | 236 Kb | |
9210A | Potentiometric Determination of Nitrate in Aqueous Samples with Ion-Selective Electrode | 122 Kb | |
9211 | Potentiometric Determination of Bromide in Aqueous Samples with Ion-Selective Electrode | 68 Kb | |
9212 | Potentiometric Determination of Chloride in Aqueous Samples with Ion-Selective Electrode | 69 Kb | |
9213 | Potentiometric Determination of Cyanide in Aqueous Samples and Distillates with Ion-Selective Electrode | 65 Kb | |
9214 | Potentiometric Determination of Fluoride in Aqueous Samples with Ion-Selective Electrode | 68 Kb | |
9215 | Potentiometric Determination of Sulfide in Aqueous Samples and Distillates with Ion-Selective Electrode | 66 Kb | |
9216 | Potentiometric Determination of Nitrite in Aqueous Samples with Ion-Selective Electrode | 126 Lb | |
9250 | Chloride (Colorimetric, Automated Ferricyanide AAI) | 206 Kb | |
9251 | Chloride (Colorimetric, Automated Ferricyanide AAII) | 204 Kb | |
9253 | Chloride (Titrimetric, Silver Nitrate) | 140 Kb | |
9310 | Gross Alpha and Gross Beta | 165 Kb | |
9315 | Alpha-Emitting Radium Isotope | 202 Kb | |
9320 | Radium-228 | 267 Kb |
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