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Métodos Analíticos EPA SERIES 8000-9000

Le ofrecemos los Métodos Analíticos más solicitados en el Análisis de Residuos. Tenga en cuenta lo siguiente:
  • Estos métodos pueden requerir adaptación a casos particulares
  • Las columnas y accesorios descritos pueden tener alternativas de superiores prestaciones
  • Nuestro Servicio Técnico le puede ayudar en cada caso
  • Podemos ofrecerle también los Estándares Certificados de Calibración,  los Materiales de Referencia requeridos para la Validación del Métodos, y la participación en Ejercicios de Intercalibración. Todos estos productos están en el apartado Estándares de este Sitio Web.
Métodos EPA Un método analítico es un procedimiento usado para analizar una muestra para determinar la identidad y concentración de un constituyente específico de la muestra. Los métodos analíticos incluyen generalmente información sobre la toma, transporte y almacenamiento de muestras; define procedimientos para concentrar, separar, identificar y cuantificar los componentes incluidos en la muestra; especifica qué criterios de control de calidad han de alcanzar los datos analíticos y especifica como construir los informes analíticos.
Muchas agencias gobernativas, universidades y organizaciones de normalización desarrollan métodos analíticos. La Environmental Protection Agency de Estados Unidos es responsable en la evaluación de cada método analítico en función de su origen. Por ejemplo la "
Office of Ground Water and Drinking Water" se responsabiliza en la evaluación de métodos analíticos desarrollados por esas organizaciones para el análisis de agua potable. La Oficina promulga, como aprobados, aquellos métodos que determina alcanzan las exigencia de la Agencia para el control de contaminantes orgánicos, inorgánicos, radio nucleares y microbiológicos. Actualmente, sólo pueden usarse métodos aprobados para el control de agua potable.
Estos métodos se entiende que se usarán como una herramienta de referencia y proveen al usuario de la información necesaria sobre métodos analíticos aprobados para el control según normativa.
EPA Serie 8000 Los Métodos de la Serie EPA 8000  ha sido diseñados para identificar contaminantes orgánicos en aguas continentales tal como prescribe la "Resource Recovery and Conservation Act (RCRA)".
Método Descripción Tamaño
8000B Determinative Chromatographic Separations 248 Kb
8010B Halogenated Volatile Organics by Gas Chromatography 150 Kb
8011 1,2-Dibromoethane and 1,2-Dibromo-3-chloropropane by Microextraction and Gas Chromatography 172 Kb
8015B Nonhalogenated Organics Using GC/FID 234 Kb
8015C Nonhalogenated Organics by Gas Chromatography 315 Kb
8020A Aromatic Volatile Organics by Gas Chromatography 165 Kb
8021B Aromatic and Halogenated Volatiles by Gas Chromatography Using Photoionization and/or Electrolytic Conductivity Detectors 130 Kb
8030A Acrolein and Acrylonitrile by Gas Chromatography 121 Kb
8031 Acrylonitrile by Gas Chromatography 77 Kb
8032A Acrylamide by Gas Chromatography 104 Kb
8033 Acetonitrile by Gas Chromatography with Nitrogen-Phosphorus Detection 73 Kb
8040

Phenols by Gas Chromatography

205 Kb
8041 Phenols by Gas Chromatography
8041A Phenols by Gas Chromatography 133 Kb
8061A Phthalate Esters by Gas Chromatography with Electron Capture Detection (GC/ECD) 103 Kb
8070A Nitrosamines by Gas Chromatography 102 Kb
8080A Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography 348 Kb
8081A Organochlorine Pesticides by Gas Chromatography 298 Kb
8081B Organochlorine Pesticides by Gas Chromatography 309 Kb
8082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography 265 Kb
8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography 376 Kb
8085 Compound-Independent Elemental Quantitation of Pesticides by Gas Chromatography with GC/AED 232 Kb
8091 Nitroaromatics and Cyclic Ketones by Gas Chromatography 116 Kb
8095 Explosives by Gas Chromatography 104 Kb
8100 Polynuclear Aromatic Hydrocarbons 207 Kb
8111 Haloethers by Gas Chromatography 87 Kb
8121 Chlorinated Hydrocarbons by Gas Chromatography: Capillary Column Technique 357 Kb
8131 Aniline and Selected Derivatives by Gas Chromatography 103 Kb
8141A Organophosphorus Compounds by Gas Chromatography: Capillary Column Technique 460 Kb
8141B Organophosphorus Compounds by Gas Chromatography 187 Kb
8151A Chlorinated Herbicides by GC Using Methylation or Pentafluorobenzylation Derivatization 228 Kb
8240B Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) 390 Kb
8260B Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) 444 Kb
8261 Volatile Organic Compounds by Vacuum Distillation in Combination with Gas Chromatography/Mass Spectrometry (VD/GC/MS) 292 Kb
8270C Semivolatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) 313 Kb
8270D Semivolatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) 374 Kb
8275A Semivolatile Organic Compounds (PAHs and PCBs) in Soils/Sludges and Solid Wastes Using Thermal Extraction/Gas Chromatography/Mass Spectrometry (TE/GC/MS) 151 Kb
8280A The Analysis of Polychlorinated Dibenzo-p-Dioxins and Polychlorinated Dibenzofurans by High Resolution Gas Chromatography/Low Resolution Mass Spectrometry (HRGC/LRMS) 269 Kb
8280B The Analysis of Polychlorinated Dibenzodioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs) by High-Resolution Gas Chromatography/Low-Resolution Mass Spectrometry (HRGC/HRMS) 172 Kb
8290 Polychlorinated Dibenzodioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs) by High-Resolution Gas Chromatography/High-Resolution Mass Spectrometry (HRGC/HRMS) 612 Kb
8290A Polychlorinated Dibenzodioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs) by High-Resolution Gas Chromatography/High-Resolution Mass Spectrometry (HRGC/HRMS) 261 Kb
8310 Polynuclear Aromatic Hydrocarbons 254 Kb
8315A Determination of Carbonyl Compounds by High Performance Liquid Chromatography (HPLC) 238 Kb
8316 Acrylamide, Acrylonitrile and Acrolein by High Performance Liquid Chromatography (HPLC) 70 Kb
8318 N-Methylcarbamates by High Performance Liquid Chromatography (HPLC) 213 Kb
8318A N-Methylcarbamates by High Performance Liquid Chromatography (HPLC) 125 Kb
8321A Solvent Extractable Nonvolatile Compounds by High Performance Liquid Chromatography/Thermospray/Mass Spectrometry (HPLC/TS/MS) or Ultraviolet (UV) Detection 239 Kb
8321B Solvent Extractable Nonvolatile Compounds by High Performance Liquid Chromatography/Thermospray/Mass Spectrometry (HPLC/TS/MS) or Ultraviolet (UV) Detection 147 Kb
8325 Solvent Extractable Nonvolatile Compounds by High Performance Liquid Chromatography/Particle Beam/Mass Spectrometry (HPLC/PB/MS) 141 Kb
8330 Nitroaromatics and Nitramines by High Performance Liquid Chromatography (HPLC) 285 Kb
8330A Nitroaromatics and Nitramines by High Performance Liquid Chromatography (HPLC) 83 Kb
8331 Tetrazene by Reverse Phase High Performance Liquid Chromatography (HPLC) 157 Kb
8332 Nitroglycerine by High Performance Liquid Chromatography 45 Kb
8410 Gas Chromatography/Fourier Transform Infrared (GC/FT-IR) Spectrometry for Semivolatile Organics: Capillary Column 210 Kb
8430 Analysis of Bis(2-chloroethyl) Ether and Hydrolysis Products by Direct Aqueous Injection GC/FT-IR 79 Kb
8440 Total Recoverable Petroleum Hydrocarbons by Infrared Spectrophotometry 48 Kb
8510 Colorimetric Screening Procedure for RDX and HMX in soil 63 Kb
8515 Colorimetric Screening Procedure for Trinitrotoluene (TNT) in soil 22 Kb
8520 Continous Measurement of Formaldehyde in Ambient Air 199 Kb
8535 Screening Procedure for Total Volatile Organic Halides in Water 86 Kb
8540 Pentachlorophenol in Soil by UV-Induced Colorimetry 73 Kb
EPA Serie 9000 Los Métodos EPA de la Serie  9000 se han diseñado para el control de contaminantes orgánicos, inorgánicos y otros parámetros en matrices varias mediante técnicas espectroscópicas.
Método Descripción Tamaño
9000 Determination of Water in Waste Materials by Karl Fischer Titration 46 Kb
9001 Determination of Water in Waste Materials by Quantitative Calcium Hydride Reaction 42 Kb
9010C Total and Amenable Cyanide: Distillation 58 Kb
9012B Total and Amenable Cyanide (Automated Colorimetric, with Off-Line Distillation) 100 Kb
9013 Cyanide Extraction Procedure for Solids and Oils 157 Kb
9014 Titrimetric and Manual Spectrophotometric Determinative Methods for Cyanide 72 Kb
9020B Total Organic Halides (TOX) 190 Kb
9021 Purgeable Organic Halides (POX) 197 Kb
9022 Total Organic Halides (TOX) by Neutron Activation Analysis 248 Kb
9023 Extractable Organic Halides (EOX) in Solids 92 Kb
9030B Acid-Soluble and Acid-Insoluble Sulfides: Distillation 113 Kb
9031 Extractable Sulfides 316 Kb
9034 Extractable Sulfides 60 Kb
9035 Sulfate (Colorimetric, Automated, Chloranilate) 215 Kb
9036 Sulfate (Colorimetric, Automated, Methylthymol Blue, AA II) 225 Kb
9038 Sulfate (Turbidimetric) 186 Kb
9040C pH Electrometric Measurement 25 Kb
9041A pH Paper Method 66 Kb
9045D Soil and Waste pH 30 Kb
9050A Specific Conductance 31 Kb
9056A Determination of Inorganic Anions by Ion Chromatography 280 Kb
9057 Determination of Chloride from HCl/Cl2 Emission Sampling Train (Methods 0050 and 0051) by Anion Chromatography 44 Kb
9060A Total Organic Carbon 26 Kb
9065 Phenolics (Spectrophotometric, Manual 4-AAP with Distillation) 212 Kb
9066 Phenolics (Colorimetric, Automated 4-AAP with Distillation) 223 Kb
9067 Phenolics (Spectrophotometric, MBTH with Distillation) 160 Kb
9070A n-Hexane Extractable Material (HEM) for Aqueous Samples 16 Kb
9071B n-Hexane Extractable Material (HEM) for Sludge, Sediment, and Solid Samples 82 Kb
9074 Turbidimetric Screening Method for Total Recoverable Petroleum Hydrocarbons in Soil 85 Kb
9075 Test Method for Total Chlorine in New and Used Petroleum Products by X-Ray Fluorescence Spectrometry (XRF) 62 Kb
9076 Test Method for Total Chlorine in New and Used Petroleum Products by Oxidative Combustion and Microcoulometry 81 Kb
9077 Test Methods for Total Chlorine in New and Used Petroleum Products (Field Test Kit Methods) 334 Kb
9078 Screening Test Method for Polychlorinated Biphenyls in Soil 32 Kb
9079 Screening Test Method for Polychlorinated Biphenyls in Transformer Oil 46 Kb
9080 Cation-Exchange Capacity of Soils (Ammonium Acetate) 266 Kb
9081 Cation-Exchange Capacity of Soils (Sodium Acetate) 135 Kb
9090A Compatibility Test for Wastes and Membrane Liners 611 Kb
9095B Paint Filter Liquids Test 28 Kb
9096 Liquid Release Test (LRT) Procedure 249 Kb
9100 Saturated Hydraulic Conductivity, Saturated Leachate Conductivity, and Intrinsic Permeability 866 Kb
9131 Total Coliform: Multiple Tube Fermentation Technique 301 Kb
9132 Total Coliform: Membrane-Filter Technique 236 Kb
9210A Potentiometric Determination of Nitrate in Aqueous Samples with Ion-Selective Electrode 122 Kb
9211 Potentiometric Determination of Bromide in Aqueous Samples with Ion-Selective Electrode 68 Kb
9212 Potentiometric Determination of Chloride in Aqueous Samples with Ion-Selective Electrode 69 Kb
9213 Potentiometric Determination of Cyanide in Aqueous Samples and Distillates with Ion-Selective Electrode 65 Kb
9214 Potentiometric Determination of Fluoride in Aqueous Samples with Ion-Selective Electrode 68 Kb
9215 Potentiometric Determination of Sulfide in Aqueous Samples and Distillates with Ion-Selective Electrode 66 Kb
9216 Potentiometric Determination of Nitrite in Aqueous Samples with Ion-Selective Electrode 126 Lb
9250 Chloride (Colorimetric, Automated Ferricyanide AAI) 206 Kb
9251 Chloride (Colorimetric, Automated Ferricyanide AAII) 204 Kb
9253 Chloride (Titrimetric, Silver Nitrate) 140 Kb
9310 Gross Alpha and Gross Beta 165 Kb
9315 Alpha-Emitting Radium Isotope 202 Kb
9320 Radium-228 267 Kb

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